Journal of Chemical Technology and Applications

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A method using dispersive solid-phase extraction (d-SPE) cleanup followed by QuEChERS with High Performance Liquid Chromatography (HPLC) has been established for determination of Neonicotinoid pesticide residues in various vegetables including brinjal, salad leaves, coriander, cabbage and woman finger. supported an assessment of the HPLC characteristics, validation experiments are conducted for 3 Neonicotinoid pesticides i.e. Nitenpyram, Imidacloprid and Acetamiprid. In acidified acetonitrile analytical extraction is completed with NaCl and MgSO4 followed by activated neutral carbon. the tactic show good linearity (R2 ≥ 0.999) and relative variance (RSD ≤ 3.36%). Average recoveries of three insecticides are within the range of 55% to 82% at spiking levels of 275.68 to 409.3 mg.Kg-1. LOD and LOQ of three Neonicotinoid pesticides are within the range of two .658 - 3.761 mg.Kg-1 and 8.056 - 11.4 mg.Kg-1. This QuEChERS determination method by HPLC is precise, simple, sensitive, accurate, easy to perform, and diversified at slightly higher concentrations. Moreover, it's very efficient and effective method and it are often utilized for normal monitoring of pesticide residues in drinking, canal and river water to save lots of the lifetime of organisms
and to stay the aquatic environment clean.

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