mass-spectrometry-congress-2019-scientifictracks

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Page 39

May 20-21, 2019 | Rome, Italy

OF EXCELLENCE

IN INTERNATIONAL

MEETINGS

YEARS

Journal of Chemical Technology and Applications | Volume 3

MASS SPECTROMETRY,

PROTEOMICS AND POLYMER CHEMISTRY

International Conference on

Mass Spectrometry Congress 2019

QUANTITATIVE ANALYSIS OF PHOSPHORUS CONTAINING NUCLEATING AGENT IN

POLYMER RESIN BY ICPMS

Birbal Bajia

and

Hemant Tyagi

Indian Oil Corporation Limited, India

eat polymer materials have poor stability and would result in a commercial failure if they are used virgin. A

nucleating agent is used in polypropylene, providing superior mechanical properties, easier dispersion and

reduced interaction with metal stearate and to give high degree of crystalline resulting in increased mechan-

ical properties such as hardness, elasticity modulus etc., and improve optical properties such as transparency

in different grade of co-polymer polypropylene virgin powder. Nucleating agent and some secondary antiox-

idants are also used which are phosphorus based. Due to common phosphorus metal in both additives it is

difficult to analyse the contribution of individual quantity as per standard test method ASTM D 6247 “Analysis

of elemental content in additive in polyolefin by X-Ray fluorescence spectrometry”. All components in combi-

nation of various additives were also not significantly separated in gas chromatography and high performance

liquid chromatography. New method developed for the analysis of nucleating agent in range of 0.01% to 0.1%

concentration. Repeatability and validation of method established.

Birbal Bajia et al., J Chem Tech App 2019, Volume 3

Birbal Bajia has completed his PhD fromMLS University, Rajasthan, India. He is the quality control manager at Indian Oil Corporation

limited, Panipat Naphtha cracker- a unit of polymer producer. He has published more than 10 papers in reputed journals and author

of three books in the field of engineering chemistry.

BIOGRAPHY